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BL22XU Large X-ray diffractometer

問い合わせ番号

INS-0000000332

Large X-ray diffractometer

 The experimental hutch 3 is located in radioisotope (RI) laboratory. X-ray diffraction measurements using coherent X-rays, resonant X-ray diffraction (mainly at K-edge of 3d transition metals, L-edge of lanthanides, and M-edge of actinides (3.5 ∼ 9 keV)) and residual stress distribution measurement, are planned. The system is designed to utilize from low energy to high energy X-rays depending upon the measurement purposes. We have a large X-ray diffractometer on which a bulky apparatus, such as a superconducting magnet, can be mounted. The diffractometer equipped with a polarization analyzer. In addition, there is a phase retarder to control the polarization of incident X-rays, and magnetic circular dichroism experiment can be performed. Sample conditions can be controlled by refrigerators (low temperature), diamond anvil cells (high pressure), and magnets (magnetic field).

Fig. 1  2-circle diffractometer with superconduction magnet

Fig. 1 2-circle diffractometer with superconduction magnet

  • Facilities for sample condition
    • He closed cycle refrigerator 1
      T > 5 K
      Diamond anvil cell can be attached.
    • He closed cycle refrigerator 2
      T > 10 K
      Pulsed magnet is attached.
    • He flow refrigerator
      T > 2 K
    • Orange cryostat
      T > 1.7 K
    • Superconducting magnet
      B < 6 T (horizontal magnetic field)
      T > 4 K
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